Yıl 2018, Cilt 14, Sayı 3, Sayfalar 327 - 331 2018-09-30

Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography

Hale Seçilmiş Canbay [1]

20 28

A sensitive method for the determination of phenothrin, promecarb and penconazole residues in tobacco has been developed. Several solvents such as, hexane, ethyl acetate and dichloromethane were tested in order to minimize agricultural products residue. In the study, the best recovery was achieved with dichloromethane. Pesticides residues are extracted from the samples with dichloromethane. Additional clean-up steps are not required for tobacco matrices. Determination and quantification of phenothrin, promecarb and penconazole are performed by gas chromatography-flame ionization detector (GC/FID) and gas chromatography-nitrogen/phosphorus (GC/NPD). The method has been validated for tobacco matrices.  Under the optimum conditions, phenothrin R2 value 0.999,   promecarb R2 value 0.999, and penconazole R2 value 0.999. Limits of determination were 0.008 µg mL-1 for phenothrin, 0.011 µg mL-1 for penconazole and 0.007 µg mL-1 for promecarb. The standard deviations (SDs) levels were in the range 0.01-0.20. Recoveries of phenothrin, promecarb and penconazole from tobacco were found to be higher than 85%. Under this developed method, the concentrations of phenothrin, promecarb and penconazole in the 10 tobacco samples were below the LOD values.
Tobacco, GC, phenothrin, promecarb, penconazole, liquid extraction
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Birincil Dil en
Konular Mühendislik
Dergi Bölümü Makaleler
Yazarlar

Orcid: 0000-0002-3783-8064
Yazar: Hale Seçilmiş Canbay (Sorumlu Yazar)
Kurum: Burdur Mehmet Akif Ersoy Üniversitesi
Ülke: Turkey


Bibtex @araştırma makalesi { cbayarfbe446820, journal = {Celal Bayar Üniversitesi Fen Bilimleri Dergisi}, issn = {1305-130X}, eissn = {1305-1385}, address = {Celal Bayar Üniversitesi}, year = {2018}, volume = {14}, pages = {327 - 331}, doi = {10.18466/cbayarfbe.446820}, title = {Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography}, key = {cite}, author = {Seçilmiş Canbay, Hale} }
APA Seçilmiş Canbay, H . (2018). Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography. Celal Bayar Üniversitesi Fen Bilimleri Dergisi, 14 (3), 327-331. DOI: 10.18466/cbayarfbe.446820
MLA Seçilmiş Canbay, H . "Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography". Celal Bayar Üniversitesi Fen Bilimleri Dergisi 14 (2018): 327-331 <http://dergipark.gov.tr/cbayarfbe/issue/39486/446820>
Chicago Seçilmiş Canbay, H . "Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography". Celal Bayar Üniversitesi Fen Bilimleri Dergisi 14 (2018): 327-331
RIS TY - JOUR T1 - Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography AU - Hale Seçilmiş Canbay Y1 - 2018 PY - 2018 N1 - doi: 10.18466/cbayarfbe.446820 DO - 10.18466/cbayarfbe.446820 T2 - Celal Bayar Üniversitesi Fen Bilimleri Dergisi JF - Journal JO - JOR SP - 327 EP - 331 VL - 14 IS - 3 SN - 1305-130X-1305-1385 M3 - doi: 10.18466/cbayarfbe.446820 UR - http://dx.doi.org/10.18466/cbayarfbe.446820 Y2 - 2018 ER -
EndNote %0 Celal Bayar Üniversitesi Fen Bilimleri Dergisi Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography %A Hale Seçilmiş Canbay %T Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography %D 2018 %J Celal Bayar Üniversitesi Fen Bilimleri Dergisi %P 1305-130X-1305-1385 %V 14 %N 3 %R doi: 10.18466/cbayarfbe.446820 %U 10.18466/cbayarfbe.446820
ISNAD Seçilmiş Canbay, Hale . "Analytical Method Development and Validation of Phenothrin, Promecarb and Penconazole in Tobacco using Liquid Extraction and Gas Chromatography". Celal Bayar Üniversitesi Fen Bilimleri Dergisi 14 / 3 (Eylül 2018): 327-331. http://dx.doi.org/10.18466/cbayarfbe.446820