Yıl 2017, Cilt 5, Sayı 4, Sayfalar 59 - 69 2017-12-22

The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte
Ultrasonik Ses Dalgası Ortamında Polielektrolit Varlığında Kalsiyum Karbonat Sentezi, Karakterizasyonu ve Deneysel Tasarım

Semra KIRBOĞA [1]

91 138

In this study, calcium carbonate (CaCO3) was synthesized by means of ultrasonic irradiation process in the presence of the water-soluble polyelectrolyte Poly(Vinyl Sulfonic Acid) (PVS). Synthesized CaCO3 crystals were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), particle size and thermal analysis (TGA-DTA). The effects of the amplitude of sonicator, polymer concentration and the application time of ultrasound on the obtained CaCO3 with respect to particle size of final product was investigated by applying the 2k Factorial design. The experimental design was studied at two levels. All the selected process parameters were found to be very effective on the particle size of calcium carbonate obtained in the presence of PVS. 

Bu çalışmada ultrasonik ses dalgası (USD) uygulanarak suda çözünebilir polielektrolit olan polivinilsülfonik asit (PVS) varlığında kalsiyum karbonat (CaCO3) sentezlenmiştir. Sentezlenen CaCO3 kristalleri XRD, taramaları elektron mikroskobu (SEM), parçacık boyutu analizi ve termogravimetrik analiz (TGA ve DTA) ile karakterize edilmiştir. 2k Faktöriyel Tasarım uygulanarak, sonikatör genliğinin, polimer konsantrasyonunun ve USD uygulama zamanının elde edilen kalsiyum karbonat kristallerinin boyutuna etkisi incelenmiştir.  Deneysel tasarım iki seviyede gerçekleştirilmiştir. Seçilen tüm proses parametrelerinin PVS varlığında elde edilen kalsiyum karbonatın parçacık boyutunda çok etkili olduğu görülmüştür.  

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Yazar: Semra KIRBOĞA (Sorumlu Yazar)
E-posta: skirboga@yildiz.edu.tr

Bibtex @araştırma makalesi { http-gujsc-gazi-edu-tr369221, journal = {Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji}, issn = {}, address = {Gazi Üniversitesi}, year = {2017}, volume = {5}, pages = {59 - 69}, doi = {10.29109/http-gujsc-gazi-edu-tr.369221}, title = {The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte}, key = {cite}, author = {KIRBOĞA, Semra} }
APA KIRBOĞA, S . (2017). The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte. Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji, 5 (4), 59-69. DOI: 10.29109/http-gujsc-gazi-edu-tr.369221
MLA KIRBOĞA, S . "The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte". Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji 5 (2017): 59-69 <http://dergipark.gov.tr/http-gujsc-gazi-edu-tr/issue/32180/369221>
Chicago KIRBOĞA, S . "The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte". Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji 5 (2017): 59-69
RIS TY - JOUR T1 - The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte AU - Semra KIRBOĞA Y1 - 2017 PY - 2017 N1 - doi: 10.29109/http-gujsc-gazi-edu-tr.369221 DO - 10.29109/http-gujsc-gazi-edu-tr.369221 T2 - Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji JF - Journal JO - JOR SP - 59 EP - 69 VL - 5 IS - 4 SN - -2147-9526 M3 - doi: 10.29109/http-gujsc-gazi-edu-tr.369221 UR - http://dx.doi.org/10.29109/http-gujsc-gazi-edu-tr.369221 Y2 - 2018 ER -
EndNote %0 Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte %A Semra KIRBOĞA %T The Synthesize of Calcium Carbonate Its Characterization and Experimental Design in an Ultrasonic Sound Wave Environment and in the Presence of Polyelectrolyte %D 2017 %J Gazi Üniversitesi Fen Bilimleri Dergisi Part C: Tasarım ve Teknoloji %P -2147-9526 %V 5 %N 4 %R doi: 10.29109/http-gujsc-gazi-edu-tr.369221 %U 10.29109/http-gujsc-gazi-edu-tr.369221